poly(styrene)



Date of Commercial Development- 1937 (Seymour 6)

Glass transition temperature- 100 deg C (Seymour 29)

Styrene monomer must be purified from trace impurities and inhibitors prior to the polymerization. This can be done either by vacuum distillation, or by purifying the monomer through an alumina chromatography column. The purified monomer is sealed under nitrogen in a glass polymerization tube and heated at 125 deg C for 1 to 7 days. The polymer contains unreacted monomer which can be removed by dissolving the polymer in benzene, and then precipitating it with methanol. A product with a molecular weight of 150,000 can be prepared this way.

[reference: Allcocke and Lampe- First edition]





Last Update- June 14, 1995- wld