Groups
A & B – Working Together:
1. Record Data from other Group.
2. At the appropriate wavelength (determined in Part A):
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a.
Zero the spectrophotometer.
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b.
Place the cuvette with the 0.5M HNO
3 in
the holder
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and
adjust the light control knob to 100%.
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Remove
the cuvette.
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c.
Place the cuvette with the solution in
the holder.
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d.
Record the % Transmittance on Datasheet
1.
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e.
Pour the solution out of the cuvette
back into the
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beaker
of ÒDiluted Fe
3+ Ó.
3. Pipet another 5.00 ml of KSCN into the beaker ![](space.gif)
of ÒDiluted Fe3+ Ó. Stir well.
4. Pour ~8 ml of solution into a cuvette.
5. Place the cuvette with the solution in the holder.
6. Record the % Transmittance on Datasheet 1.
7. Pour the solution out of the cuvette back
into the beaker of ÒDiluted Fe3+ Ó.
8. Repeat steps 14-18 to obtain the remaining data.