1. Fill sample vapor only in syringe (NOT liquid!).
2. Overfill
syringe then adjust to desired amount.
3. Do not let the
sample remain in the syringe long before
injecting to avoid vapor loss into
the rubber plunger of
the
syringe.
4. Rotate the
syringe when
piercing the latex tubing to avoid
a pressure surge which may
blow out the flame.
5. Inject as
close as possible to the column head.
6. Push the
plunger fairly rapidly during injection.
7.
Chloroform (CHCl3 )
may require a larger amount
than
suggested to get adequate sensor response