Experimental Apparatus for Measuring Gas Desorption and Pico-gram Mass Changes in Nano-scale Metal-hydrogen Systems Confined in Nano-porous Frameworks

David Peaslee
University of Missouri - St. Louis
Majzoub Research Group


Abstract
Thermodynamic properties of metal hydrides differ between bulk and nano-sized particles. By adjusting the size of these particles and confining them in nano-porous materials, properties including the hydrogen desorption and adsorption temperature can be fine-tuned to meet engineering requirements for real-world systems. The combined residual gas analyzer mass spectrometer (RGAMS) and quartz crystal microbalance (QCM) system can be used to characterize gas desorption, decomposition temperatures, picogram changes in mass, and ionization energies for a variety of materials systems. The description of the processes and recent data collected will be discussed here.
David Peaslee is a California native attending the University of Missouri - St. Louis. He graduated with a B.S. in Physics and a B.A. in Mathematics in 2007 from UMSL. He earned his M.S. in physics in 2008 and is presently a PhD student working as a research assistant with Dr. Eric Majzoub's material science research group.
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